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Beilstein J. Org. Chem. 2009, 5, No. 16, doi:10.3762/bjoc.5.16
Graphical Abstract
Scheme 1: Sequential introduction of two electrophiles onto dibromobiaryls using Br-Li exchange reactions.
Scheme 2: Br-Li exchange reaction of 2,2′-dibromobiphenyl (1) with n-BuLi using a conventional macrobatch rea...
Figure 1: Microflow system for Br-Li exchange reaction of 2,2′-dibromobiphenyl (1). T-shaped micromixer: M1 (...
Figure 2: Effect of temperature and residence time in Br-Li exchange reaction of 2,2′-dibromobiphenyl (1) usi...
Figure 3: A microflow system for sequential introduction of two electrophiles. T-shaped micromixer: M1 (ø = 2...
Scheme 3: Br-Li exchange reaction of 4,4′-dibromobiphenyl (17) with n-BuLi using a conventional macrobatch re...
Figure 4: Microflow system for Br-Li exchange reaction of 4,4′-dibromobiphenyl (17). T-shaped micromixer: M1 ...
Figure 5: Effect of temperature and residence time in Br-Li exchange reaction of 4,4′-dibromobiphenyl (17) us...